# 1 "/u/exp/stan/nmr/lists/pp/inv4gslplrnd" ;inv4gslplrnd ;avance-version ;2D H-1/X correlation via heteronuclear zero and double quantum ; coherence ;optimized on long range couplings ;with low-pass J-filter to suppress one-bond correlations ;no decoupling during acquisition ;using gradient pulses for selection # 1 "/u/exp/stan/nmr/lists/pp//Avance.incl" ;Avance.incl ; ;version 99/08/02 # 12 "/u/exp/stan/nmr/lists/pp/inv4gslplrnd" # 1 "/u/exp/stan/nmr/lists/pp//Grad.incl" ;Grad.incl - include file for Gradient Spectroscopy ;avance-version ;version 99/02/19 define list EA= # 13 "/u/exp/stan/nmr/lists/pp/inv4gslplrnd" "p2=p1*2" "d0=3u" "d2=1s/(cnst2*2)" "d13=3u" 1 ze 2 d1 3 p1 ph1 d2 p3:f2 ph3 d6 p3:f2 ph4 d0 50u setnmr2|0 setnmr0|34 p16:ngrad:c34 d16 p2 ph2 50u p16:ngrad:c34 d16 d0 p3:f2 ph5 d13 p16:ngrad:c34 d16 4u setnmr2^0 setnmr0^34 go=2 ph31 d1 do:f2 wr #0 if #0 id0 zd lo to 3 times td1 exit ph1=0 ph2=0 0 0 0 2 2 2 2 ph3=0 0 2 2 ph4=0 2 ph5=0 0 0 0 0 0 0 0 2 2 2 2 2 2 2 2 ph31=0 2 0 2 0 2 0 2 2 0 2 0 2 0 2 0 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J)XH ;d6 : delay for evolution of long range couplings ;d13: short delay [3 usec] ;d16: delay for homospoil/gradient recovery ;cnst2: = J(XH) ;in0: 1/(2 * SW(X)) = DW(X) ;nd0: 2 ;NS: 2 * n ;DS: 16 ;td1: number of experiments ;MC2: QF ;use gradient program (GRDPROG) : 3sine ;use gradient ratio: cnst21 : cnst22 : cnst23 ; 50 : 30 : 40 for C-13 ; 70 : 30 : 50 for N-15